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Preparation and characterization of sterically protected primary phosphine sulfide and oxide

โœ Scribed by Masaaki Yoshifuji; Katsuhiro Shibayama; Kozo Toyota; Naoki Inamoto

Publisher
Elsevier Science
Year
1983
Tongue
French
Weight
133 KB
Volume
24
Category
Article
ISSN
0040-4039

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โœฆ Synopsis

Sterically protected primary phosphine sulfide (l) and oxide (a, were prepared from 2,4,6-tri-tert-butylphenylphosphine (2) and were characterized as stable compounds.

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## Abstract The hydrolytic stability of the sterically protected dichlorosilane (Mes\*๏ฃฟO)~2~SiCl~2~ was investigated. The resulting products have been identified by electrospray mass spectrometry and, in the case of (Mes\*๏ฃฟO)~2~Si(OH)~2~, the crystal structure was obtained. Copyright ยฉ 2005 John Wi