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Practicalities and applications of reverse heteronuclear shift correlation: Porphyrin and polysaccharide examples

✍ Scribed by John Cavanagh; Christopher A. Hunter; David N. M. Jones; James Keeler; Jeremy K. M. Sanders

Book ID
102950137
Publisher
John Wiley and Sons
Year
1988
Tongue
English
Weight
975 KB
Volume
26
Category
Article
ISSN
0749-1581

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✦ Synopsis

The practical aspects of protondetected heteronuclear shift correlation spectroscopy are described in detail, with emphasis on the precautions necessary to obtain efficient suppression of signals from protons that are not coupled to 13C. The experiment has been used to assign the quaternary carbon signals of a porphyrin and to resolve the proton spectrum of the K 3 serotype polysaccharide.

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