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Positive chemical ionization and tandem mass spectrometric fragmentation for the gas chromatographic analysis ofβ-agonists using the ion trap technique

✍ Scribed by Biancotto, Giancarlo; Angeletti, Roberto; Traldi, Pietro; Guidugli, Federico

Publisher
John Wiley and Sons
Year
1999
Tongue
English
Weight
158 KB
Volume
34
Category
Article
ISSN
1076-5174

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✦ Synopsis

A procedure is described for the determination of three characteristic b-agonists (clenbuterol, terbutalin and salbutamol) based on the formation of the corresponding protonated molecules and related collisional experiments. Quantification was carried out on selected collisional fragments and the reproducibility of the relative abundances of these fragments was estimated. The performance of the method was tested on bovine urine samples spiked at the lowest level of 0.2 ng ml -1 in each of the chosen compounds.

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