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Polysiloxane deactivated fused silica capillaries containing immobilized stationary phases

✍ Scribed by Moseley, M. A. ;Pellizzari, E. D.

Book ID
102347006
Publisher
John Wiley and Sons
Year
1982
Tongue
English
Weight
307 KB
Volume
5
Category
Article
ISSN
0935-6304

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✦ Synopsis

Abstract

This article describes a method of preparing immobilized stationary phases which has arisen from the authors' work on polysiloxane deactivation of fused silica capillaries. Although acid treatment is often omitted with fused silica capillaries, there are good reasons for hydrothermal treatment of this column material. Use of Grob's peroxide method gave immobilized 0.25 ΞΌm films of SE‐54; lowering of the immobilization temperature permitted immobilization of 0.1 ΞΌm films of the same phase.

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