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Polymeric (ethyl­enedi­amine)silver(I) 2,4,6-tri­nitro­phenolate

✍ Scribed by Zhu, Hai-Liang ;Wang, Xian-Jiang ;Meng, Fan-Jin ;Liu, Xiu-Ying

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
291 KB
Volume
59
Category
Article
ISSN
1600-5368

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✦ Synopsis

The asymmetric unit of the title compound, (I), showing 50% probability displacement ellipsoids and the atom-numbering scheme.

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The 1:2 adduct N,N-di­methyl­ethyl­enedi
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Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.005 A Ê R factor = 0.058 wR factor = 0.138 Data-to-parameter ratio = 11.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

A polymeric tetraimine Schiff base macro
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Silver(I)-templated cyclocondensation of pyridine-2,6\_dicarbaldehyde and 3-oxa-1,5-diammopentane yields a dinuclear silver(I) complex of the '2+2' tetraimine Schiff base macrocycle L,. The crystal structure of the complex recrystallised from acetonitrile shows the product of recrystallisation to be