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Photopolymer: synthesis and characterization of poly(4-methacryloyloxyphenyl-4′-chlorostyryl ketone)

✍ Scribed by K Subramanian; V Krishnasamy; S Nanjundan; A V Rami Reddy

Publisher
John Wiley and Sons
Year
2000
Tongue
English
Weight
153 KB
Volume
49
Category
Article
ISSN
0959-8103

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✦ Synopsis

Methacrylate monomer containing a photodimerizable a,b-unsaturated ketone moiety was prepared and polymerized in ethyl methyl ketone at 70 °C using benzoyl peroxide as an initiator. The polymer was characterized by UV, IR, 1 H NMR and 13 C NMR spectra. The molecular weights (M w and M n ) of the polymer were determined by gel permeation chromotography. The thermal stability of the polymer was measured by thermogravimetric analysis in air and nitrogen. The glass transition temperature of the polymer was determined by differential scanning calorimetry. The photo reactivity of the polymer was investigated as thin ®lm and in solution.

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