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Photolysis of the cyclopentadienyl(hydrido) Complexes C5H5M(CO)3H (M = Cr, Mo, W) in Matrices and in Solution: Characterization of [C5H5W(CO)2H]2 and [C5Me5W(CO)2H]2

✍ Scribed by Priv.-Doz. Dr. Helmut G. Alt; Khalil A. Mahmoud; Dr. Antony J. Rest

Publisher
John Wiley and Sons
Year
1983
Tongue
English
Weight
244 KB
Volume
22
Category
Article
ISSN
0044-8249

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The anionic clusters [Fe 5 MN(CO) 14 Cp] 2-[M = Mo (1) or W (2)] were synthesized from [Fe 4 N(CO) 12 ] -and [MCp(CO) 3 ] - in refluxing acetonitrile. The clusters [Fe 3 M 3 N(CO) 18 ] 3-[M = Mo (3) or W (4)] were prepared by reaction of [Fe 4 N(CO) 12 ] - with [M 2 (CO) 10 ] 2-under the same condit