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Photolysis of organopolysilanes. The reaction of photochemically generated methylphenylsilylene with conjugated dienes

✍ Scribed by Mitsuo Ishikawa; Ken-Ichi Nakagawa; Ryuichi Enokida; Makoto Kumada

Book ID
108354098
Publisher
Elsevier Science
Year
1980
Tongue
English
Weight
843 KB
Volume
201
Category
Article
ISSN
0022-328X

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CF 3 O 2 CF 3 was photolyzed at 254 nm in the presence of CO in 760 torr N 2 or air at 296 K in a static reactor. In N 2 , the products CF 3 OC(O)C(O)OCF 3 and CF 3 OC(O)O 2 C(O)OCF 3 were detected by FTIR spectroscopy. In air, the only observed products were CF 2 O and CO 2 and a chain process, ini