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Photochemistry of bioactive compounds. Solution-phase photochemistry of asymmetric triazin-5 (4H)-ones

✍ Scribed by Pape, Brian E.; Zabik, Matthew J.

Book ID: 126941265
Publisher: American Chemical Society
Year: 1972
Tongue: English
Weight: 395 KB
Volume: 20
Category: Article
ISSN: 0021-8561
DOI: 10.1021/jf60179a020

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A new and easy protocol for the formation of substituted 4,5-dihydro-1,2,4-triazin-6(1H)-ones was developed on solid support. The heterocyclic compounds were formed by nucleophilic reaction of hydrazine on thioamide esters. As cyclization was concomitant with cleavage from the support, substituted 4