E, they are also not hydrolyzed by conc. hydrochloric acid. 3a-c can be deprotonated with sodium hydroxide and acylated at the nitrogen. Although in the 1,2,4-diazaphospholes a 1,3-diamino-2phosphaallyl system is still formally present, the ring closure is associated with an essential change: the c
Photochemical Synthesis of a (η4-Diene)(η2-Olefin)Fe(CO)2 Complex and Subsequent Thermal Coupling of the Ligands
✍ Scribed by Dr. Friedrich-Wilhelm Grevels; Konrad Schneider
- Publisher
- John Wiley and Sons
- Year
- 1981
- Tongue
- English
- Weight
- 211 KB
- Volume
- 20
- Category
- Article
- ISSN
- 0044-8249
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
## Experimental Section 3: Compound 4 [4] (80 mg, 0.075 mmol) and KC 8 (22 mg, 0.163 mmol) were placed in a reaction tube with a magnetic stirrer. Oxygen-free, dry THF (2 mL) was introduced into the reaction tube by vacuum transfer, and the reaction mixture was stirred at room temperature to produ
Section 3: Compound 4 [4] (80 mg, 0.075 mmol) and KC 8 (22 mg, 0.163 mmol) were placed in a reaction tube with a magnetic stirrer. Oxygen-free, dry THF (2 mL) was introduced into the reaction tube by vacuum transfer, and the reaction mixture was stirred at room temperature to produce a yellow soluti