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Photocatalytic initiation of thiol–ene reactions: synthesis of thiomorpholin-3-ones

✍ Scribed by Keylor, Mitchell H.; Park, James E.; Wallentin, Carl-Johan; Stephenson, Corey R.J.

Book ID
121833091
Publisher
Elsevier Science
Year
2014
Tongue
French
Weight
697 KB
Volume
70
Category
Article
ISSN
0040-4020

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Solid phase synthesis of 2,4,5-trisubsti
Solid phase synthesis of 2,4,5-trisubstituted thiomorpholin-3-ones
✍ Adel Nefzi; Marc Giulianotti; Richard A. Houghten 📂 Article 📅 1998 🏛 Elsevier Science 🌐 French ⚖ 170 KB

The solid phase synthesis of 2,4,5-trisubstituted thiomorpholin-3-ones is described. Starting from a resin-bound protected cysteine, and employing reductive alkylation and amide formation, thiomoq~holin-3one derivatives have been synthesized through intramolecular thioether formation in good yield a