Phosphorus(V) Nitride Imide HP4N7: Synthesis from a Molecular Precursor and Structure Determination with Synchrotron Powder diffraction

ChemInform Abstract: Phosphorus(V)-nitri

ChemInform Abstract: Phosphorus(V)-nitridimide HP4N7: Synthesis from a Molecular Precursor and Powder X-Ray Analysis with Synchroton Radiation.

✍ S. HORSTMANN; E. IRRAN; W. SCHNICK 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 30 KB

Phosphorus(V)-nitridimide HP4N7: Synthesis from a Molecular Precursor and Powder X-Ray Analysis with Synchroton Radiation. -Phase pure HP4N7 is obtained as microcrystalline powder in 76.3% yield by pyrolysis of (NH2)2P(S)NP(NH2)3 at 750 • C (sealed quartz ampoule, Ar). According to the powder synch