✦ LIBER ✦

Phosphorus Pentoxide in Organic Synthesis, XVI. A One-step Synthesis of 2-Methyl-N6-aryladenines from 5-Acetylamino-1H-imidazole-4-carboxamide Hydrochloride

✍ Scribed by Andersen, Knud Erik ;Pedersen, Erik B.

Publisher: John Wiley and Sons
Year: 1985
Tongue: English
Weight: 316 KB
Volume: 1985
Category: Article
ISSN: 0947-3440
DOI: 10.1002/jlac.198519850506

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✦ Synopsis

Abstract

5‐Amino‐1__H__‐imidazole‐4‐carboxamide hydrochloride has been converted into a series of 2‐methyl‐6‐(arylamino)purines 3 via 5‐acetylamino‐1__H__‐imidazole‐4‐carboxamide hydrochloride (1) which was heated with phosphorus pentoxide, triethylamine hydrochloride, and an appropriate substituted aniline at 180°C.

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