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Phase change and thermochromism of crystalline 2,4-dihydroxybenzylidene-4-aminoantipyrine and its UO2(VI) complex in the solid state

✍ Scribed by F.A. El-Saied; M.M. Ayad; M.I. Ayad

Publisher
Elsevier Science
Year
1990
Tongue
English
Weight
439 KB
Volume
165
Category
Article
ISSN
0040-6031

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✍ M. V. Galakhov; V. I. Bakhmutov; I. V. Barinov 📂 Article 📅 1991 🏛 John Wiley and Sons 🌐 English ⚖ 180 KB

## Abstract Internal rotation about the C‐2–C‐3 bond was observed in the ^13^C CP‐MAS NMR spectra of the solid complexes [M~2~(ηHC^1^C^2^C^3^Me~2~)(CO)~4~(ηC~5~H~5~)~2~]^+^ [BF~4~]^−^ where M = Mo or W.