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Peroxo malato vanadates(V): syntheses, spectra and structure of the (NH4)2[VO(O2)(C4H4O5)]22H2O dimer with a rhomboidal V2O2(hydroxyl) bridging core

โœ Scribed by C Djordjevic; M Lee-Renslo; E Sinn

Publisher
Elsevier Science
Year
1995
Tongue
English
Weight
712 KB
Volume
233
Category
Article
ISSN
0020-1693

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Hydrothermal Syntheses and Structures of
Hydrothermal Syntheses and Structures of Three-Dimensional Oxo-fluorovanadium Phosphates: [H2N(C2H4)2NH2]0.5[(VO)4V(HPO4)2(PO4)2F2(H2O)4] ยท 2H2O and K2[(VO)3(PO4)2F2(H2O)] ยท H2O
โœ Grant Bonavia; R.C Haushalter; Jon Zubieta ๐Ÿ“‚ Article ๐Ÿ“… 1996 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 420 KB

2.5 , monoclinic C2/m, a โ€ซุโ€ฌ 18.425(4) A หš, c โ€ซุโ€ฌ 8.954(2) A หš, โค โ€ซุโ€ฌ 93.69(2) 0 , V โ€ซุโ€ฌ 1221.1(4) A หš3, Z โ€ซุโ€ฌ 4, D calc โ€ซุโ€ฌ 2.423 g cm ุŠ3 ; 2 ุ’ H 2 O, H 4 F 2 K 2 O 13 P 2 V 3 , triclinic P1, a โ€ซุโ€ฌ 7.298(1) A หš, b โ€ซุโ€ฌ 8.929(2) A หš, c โ€ซุโ€ฌ 10.090(2) A หš, โฃ โ€ซุโ€ฌ 104.50(2) 0 , โค โ€ซุโ€ฌ 100.39(2) 0 , โฆ โ€ซุโ€ฌ

The Hydrothermal NH4/V/P/H2O and K/V/P/N
The Hydrothermal NH4/V/P/H2O and K/V/P/N(C2H5)3/H2O Systems at 473 K and the Crystal Structures of NH4VOPO4and (NH4)3V2O3(VO)(PO4)2(HPO4)
โœ Michael Schindler; Werner Joswig; Werner H. Baur ๐Ÿ“‚ Article ๐Ÿ“… 1997 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 333 KB

4ุ‰ , and As 5ุ‰ , but none of them crystallize in space group Pn2n. In the K/V/P/N(C 2 H 5 ) 3 / H 2 O system, three different K phases were found: K 0.5 VOPO 4 โ€ข 1.5H 2 O, KVOPO 4 , and K-FVP-1 (Frankfurt vanadium phosphate, one, or for short, FVP-1). The microporous K-FVP-1 compound was synthesize