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Hydrothermal Syntheses and Structures of Three-Dimensional Oxo-fluorovanadium Phosphates: [H2N(C2H4)2NH2]0.5[(VO)4V(HPO4)2(PO4)2F2(H2O)4] · 2H2O and K2[(VO)3(PO4)2F2(H2O)] · H2O

✍ Scribed by Grant Bonavia; R.C Haushalter; Jon Zubieta

Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
420 KB
Volume
126
Category
Article
ISSN
0022-4596

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✦ Synopsis

2.5 , monoclinic C2/m, a ‫؍‬ 18.425(4) A ˚, c ‫؍‬ 8.954(2) A ˚, ␤ ‫؍‬ 93.69(2) 0 , V ‫؍‬ 1221.1(4) A ˚3, Z ‫؍‬ 4, D calc ‫؍‬ 2.423 g cm ؊3 ; 2 ؒ H 2 O, H 4 F 2 K 2 O 13 P 2 V 3 , triclinic P1, a ‫؍‬ 7.298(1) A ˚, b ‫؍‬ 8.929(2) A ˚, c ‫؍‬ 10.090(2) A ˚, ␣ ‫؍‬ 104.50(2) 0 , ␤ ‫؍‬ 100.39(2) 0 , ␦ ‫؍‬ 92.13(2) 0 , V ‫؍‬ 623.8(3) A ˚3, Z ‫؍‬ 2, D calc ‫؍‬ 2.891 g cm ؊3 .

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