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Perhydro-1,3-diazepine-2,4-diones by cyclization of 4-ureidobutyric acids with thionyl chloride: A reinvestigation

✍ Scribed by Roland Heckendorn; Tammo Winkler


Publisher
Journal of Heterocyclic Chemistry
Year
2000
Tongue
English
Weight
187 KB
Volume
37
Category
Article
ISSN
0022-152X

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✦ Synopsis


Abstract

The structures of the previously reported aryl‐perhydro‐1,3‐diazepine‐2,4‐diones are shown to be pyrro‐lidinone carboxamide derivatives by nmr spectroscopy.


📜 SIMILAR VOLUMES


Synthesis of new 6-(4-chlorophenyl)perhy
✍ Jean Guillon; Pascal Sonnet; Patrick Dallemagne; Hugues Miel; Sylvain Rault; Mar 📂 Article 📅 1998 🏛 Journal of Heterocyclic Chemistry 🌐 English ⚖ 371 KB

## Abstract Synthesis of new 6‐(4‐chlorophenyl)perhydro‐1,3‐diazepine‐2,4‐diones was accomplished starting from 4‐amino‐3‐(4‐chlorophenyl)butyric acid (Baclofen). The chemical pathway involved the cyclisation of various 3‐(4‐chlorophenyl)‐4‐ureidobutyric acids. However, none of the new derivatives