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Perfluoroalkylation of 2-Thiopyrimidine Derivatives.

✍ Scribed by A. M. Sipyagin; V. S. Enshov

Publisher
John Wiley and Sons
Year
2004
Weight
88 KB
Volume
35
Category
Article
ISSN
0931-7597

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Dithionite-mediated perfluoroalkylation
Dithionite-mediated perfluoroalkylation of furan derivatives with dimerization
✍ Stefan Tews; Martin Hein; Ralf Miethchen πŸ“‚ Article πŸ“… 2002 πŸ› Elsevier Science 🌐 French βš– 166 KB

2,5-Dimethylfuran (1) and 2-pivaloyloxymethylfuran (4) were alkylated with 1-iodo-perfluorohexane using sodium dithionite as radical initiator. Perfluorohexylation in the 2-position accompanied with dimerization was observed forming the products 2, 3 and 5, respectively.