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Peptide studies using a fast atom bombardment high field mass spectrometer and data system: 3—negative ionization: Mass calibration, data acquisition and structural characterization

✍ Scribed by Alexander M. Buko; Lawrence R. Phillips; Blair A. Fraser

Publisher
John Wiley and Sons
Year
1983
Tongue
English
Weight
483 KB
Volume
10
Category
Article
ISSN
1076-5174

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Peptide studies using a fast atom bombar
Peptide studies using a fast atom bombardment high field mass spectrometer and data system. 1—Sample introduction, data acquisition and mass calibration
✍ Alexander M. Buko; Lawrence R. Phillips; Blair A. Fraser 📂 Article 📅 1983 🏛 John Wiley and Sons 🌐 English ⚖ 952 KB

Conditions were established for analyzing as little as 5 pmol of an underivatized peptide delivered in a glycerol sample matrix as a thin film onto a gold-plated copper sample stage and then bombarded with xenon fast atoms. Calibration of the fast atom bombardment high field mass spectrometer and da

Peptide studies using a fast atom bombar
Peptide studies using a fast atom bombardment high field mass spectrometer and data system. 4. Disulfide-containing peptides
✍ Alexander M. Buko; Blair A. Fraser 📂 Article 📅 1985 🏛 John Wiley and Sons 🌐 English

Ten peptides containing one, two or three disulfides were examined to determine their behavior under fast atom bombardment (FAB) mass spectrometric conditions. The mass spectra for the disulfide and the reduced disulfide forms of each peptide were compared. Several factors were examined that contrib