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Partial asymmetric synthesis in the Simmons-Smith reaction. I

✍ Scribed by Sawada, S.; Takehana, K.; Inouye, Y.

Book ID: 111900210
Publisher: American Chemical Society
Year: 1968
Tongue: English
Weight: 519 KB
Volume: 33
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo01269a014

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Alkenylsilanols and the corresponding lithium silanolates prepared in situ by the reaction of cyclic siloxanes with alkenyllithiums are transformed to the corresponding cyclopropylsilanols under the Simmons-Smith reaction conditions. The obtained cyclopropylsilanols are further converted into the co