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Parallel synthesis of benzoxazoles via microwave-assisted dielectric heating

โœ Scribed by Richard S. Pottorf; Naresh K. Chadha; Martins Katkevics; Vita Ozola; Edgars Suna; Hadi Ghane; Tor Regberg; Mark R. Player


Book ID
104252606
Publisher
Elsevier Science
Year
2003
Tongue
French
Weight
263 KB
Volume
44
Category
Article
ISSN
0040-4039

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Microwave-assisted solvent-free parallel
โœ Roger Olsson; Henrik C Hansen; Carl-Magnus Andersson ๐Ÿ“‚ Article ๐Ÿ“… 2000 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 58 KB

Rapid parallel synthesis of thioamides is described. A library of amides, synthesised by mixing acyl chlorides and diamines, was transformed into the corresponding thioamides utilising Lawesson's reagent as the oxygen/sulphur exchange reagent. Purification by solid-phase extraction afforded the libr