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Palladium(II) catalyzed carbonylative dimerization of allenyl ketones: efficient synthesis of difuranylketones

✍ Scribed by Keisuke Kato; Tomoyuki Mochida; Hiroyuki Takayama; Masayuki Kimura; Hiroshi Moriyama; Akihito Takeshita; Yuichro Kanno; Yoshio Inouye; Hiroyuki Akita

Publisher
Elsevier Science
Year
2009
Tongue
French
Weight
320 KB
Volume
50
Category
Article
ISSN
0040-4039

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Cyclic ketones react with PdCl 2 in methanol under a CO atmosphere to give mainly diesters by a ring cleavage reaction along with some chloro-substituted monoester. 13 CO labeling experiments indicate the major product is formed by a mechanism involving Pd(II)-CO 2 CH 3 insertion across the double b