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Palladium-catalyzed carbonylative cyclization of 3-bromoallyl alcohols leading to furan-2(5H)-ones

✍ Scribed by Hye Kyung Lee; Chan Sik Cho

Book ID
112001511
Publisher
John Wiley and Sons
Year
2012
Tongue
English
Weight
222 KB
Volume
26
Category
Article
ISSN
0268-2605

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a b s t r a c t 2-Bromobenzaldehyde is carbonylatively cyclized with primary amines under carbon monoxide pressure in DMF at 100 Β°C in the presence of a catalytic amount of a palladium catalyst to give the corresponding isoindolin-1-ones in moderate to high yields.

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## Abstract 2‐Bromobenzaldehyde reacts with an excess of primary amines under a carbon monoxide in the presence of a catalytic amount of bis(triphenylphosphine)palladium(II) chloride together with triethylamine to give the corresponding 3‐(alkylamino)isoindolin‐1‐ones in good yields.