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Palladium-Catalyzed Base-Selective H—D Exchange Reaction of Nucleosides in Deuterium Oxide.

✍ Scribed by Hironao Sajiki; Hiroyoshi Esaki; Fumiyo Aoki; Tomohiro Maegawa; Kosaku Hirota

Publisher
John Wiley and Sons
Year
2005
Weight
21 KB
Volume
36
Category
Article
ISSN
0931-7597

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## Abstract The Pd/C‐catalyzed H~2~–D~2~ exchange reaction using a H~2~–D~2~O combination provided a general, efficient and environmentally friendly route for the preparation of deuterium gas (D~2~). H~2~ sealed in a reaction flask was converted into nearly pure D~2~, which could be used for the Pd