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P-N compounds. 25. Phosphaminimides. 1. Synthesis and bioevaluation of a derivative of tetrahydro-2H-1,3,4,2-oxadiazaphosphorinium inner salt

โœ Scribed by Lindley A. Cates; Ven-Shun Li; Jyoti P. Basrur; Bashir H. Saddawi; Karim A. Alkadhi


Book ID
112127760
Publisher
Journal of Heterocyclic Chemistry
Year
1985
Tongue
English
Weight
203 KB
Volume
22
Category
Article
ISSN
0022-152X

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Tic palladium-catalyzed intramolecular cyclization of l-butyl-l(o-iodobenzyl)-3-pheaylurea 1 at gOยฐC m the Ixesence of carbon monoxide at atmospheric pressure gives the corresl~nding 2,3,4,5-teWahydro-IH-2,4benzodiazepine-1,3-dione derivative 2 in 91% yield. Yield and selectivity are strongly affect