✦ LIBER ✦

Oxygen Complexes of Zerovalent Nickel, Palladium, and Platinum

✍ Scribed by Prof. Dr. G. Wilke; Dr. H. Schott; Dr. P. Heimbach

Publisher: John Wiley and Sons
Year: 1967
Tongue: English
Weight: 240 KB
Volume: 6
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.196700921

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✦ Synopsis

gave a value of 297. (The preparation of (CH3CN)3Cr(C0)3 was as described by Tare [41.) Reaction conditions: stirring at 30 "C and 1 5 mm/Hg for some hours. Table 1. Comparison of tricarbonylhexamethyiborazolechromiurn with a typical rr-complex and a Lewis-base complex Appearance Behaviour in high vacuum Decomposition temperature( OC Stability in air Solubility in benzene v(C0) (cm-1) UV Maxima in C6H12 Y (cm-I); log E Dipole moment in benzene (D) orange-yellow needles sublimes at 90 O C without decamp. 141 days readily soluble 1867 in C6H12 1963 [ml 25320 3.65 36760 Lshl 3.78 46080 4.37 7.24 rt 0.05 yellow crystals sublimes at 90 "C without decornp.

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