Addition of water to the reaction mixture also eliminates this peak, suggesting that a reaction with water may displace one or more of the trimethylsilyl groups. This more labile component can be restored by retreatment with trimethylchlorosilane and hexamethyldisilazane. An explanation for these tw
Oxygen bomb combustion of environmental and biological samples for tritium analysis
โ Scribed by A.A. Moghissi; E.W. Bretthauer; E.L. Whittaker; D.N. McNelis
- Publisher
- Elsevier Science
- Year
- 1975
- Weight
- 252 KB
- Volume
- 26
- Category
- Article
- ISSN
- 0020-708X
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๐ SIMILAR VOLUMES
An analytical procedure, oxygen bomb combustion ion chromatography (IC), was developed for the elemental analysis of heteroatoms in fuel and organic wastes. The use of oxygen bomb combustion under elevated oxygen pressure (25 atm) was shown to produce nitrate upon oxidation of atmospheric nitrogen.
For the analysis of biological and environmental materials by inductively coupled plasma mass spectrometry (ICP-MS), several quantiรcation procedures can be used depending on the precision and accuracy required. Semiquantitative methods based on the molar response curve were compared with convention