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Oxidation of benzoic acid-1-14C to phenol

✍ Scribed by W. Schoo; J. U. Veenland; J. A. Bigot; F. L. J. Sixma

Publisher
Elsevier Science
Year
2010
Tongue
English
Weight
214 KB
Volume
80
Category
Article
ISSN
0165-0513

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✦ Synopsis

Abstract

Using benzoic acid‐1‐^14^C the position of the hydroxyl group formed in the oxidation of benzoic acid to phenol and carbon dioxide is definitively identified as ortho in relation to the original carboxyl group.

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✍ D. Georgin; S. de Suzzoni-Dezard; J. P. Noel πŸ“‚ Article πŸ“… 1996 πŸ› John Wiley and Sons 🌐 French βš– 282 KB πŸ‘ 1 views

The preparation of [U-14C] 2,4-dichlorophenol was formerly achieved by a Sandmeyer reaction with p-'4C] 2,4-dichloroaniline but this sensitive step gave unreproductive yields in our hands. We describe another route to [U-I4C] 2,4-dichlorophenol by the oxidative chlorination of !J.J-I4C] phenol. Thi