The reaction of dibutyltin oxide with Schiff bases derived from sulpha drugs in 1:1 molar ratio leads to the formation of a new series of organotin(IV) complexes. An attempt has been made to probe their structure on the basis of UV, IR, NMR ( 1 H, 13 C and 119 Sn) and Mo ¨ssbauer spectral studies. A
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Organotin-Drug Interactions. Organotin Adducts of Tenoxicam: Synthesis and Characterization of the First Organotin Complex of Tenoxicam
✍ Scribed by Mavroudis A. Demertzis; Sotiris K. Hadjikakou; Dimitra Kovala-Demertzi; Aglaia Koutsodimou; Maciej Kubicki
- Publisher
- John Wiley and Sons
- Year
- 2000
- Tongue
- German
- Weight
- 219 KB
- Volume
- 83
- Category
- Article
- ISSN
- 0018-019X
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All reagents were of analytical grade and were used without further purification. R 3 SnCl (R = Me, n-Bu, C 6 H 11 and Ph) were of commercial origin; (PhCH 2 ) n SnCl 4 Ϫ n (n = 1, 2) were prepared by literature methods. Solvents were dried by standard procedures. Spectra were recorded on the foll