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Organocatalytic Synthesis of N -Phenylisoxazolidin-5-ones and a One-Pot Synthesis of β-Amino Acid Esters

✍ Scribed by Seayad, Jayasree; Patra, Pranab Kumar; Zhang, Yugen; Ying, Jackie Y.

Book ID
126298446
Publisher
American Chemical Society
Year
2008
Tongue
English
Weight
99 KB
Volume
10
Category
Article
ISSN
1523-7060

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Mono-N-ethylated h-amino acid esters are obtained in high yields using reductive amination procedures. Formation of imine is achieved by excess of acetaldehyde, followed by removal of acetaldehyde and reduction by NaBH(OAc) 3 . The elaborated one-pot synthesis allows for the efficient synthesis of s