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Organoboron Compounds. XVI. An Improved Method for the Preparation of Trialkylboroxines 1,2

✍ Scribed by McCusker, Patrick A.; Bright, John H.

Book ID
127146322
Publisher
American Chemical Society
Year
1964
Tongue
English
Weight
301 KB
Volume
29
Category
Article
ISSN
0022-3263

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A simple and fast route for the preparation of 1,2-isopropylidene-sn-glycerol from Dmannitol in 45% yield is described. The value of optical rotation, [a] ~ + 15.2 Β°, is higher than usual indicating considerable racemization for other procedures, Since 1,2-isopropylidene-sn-glycerol serves as genera