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Organic Reactions with Silicon Compounds. 1 II. The Reaction of Silicon Tetrafluoride with the Grignard Reagent

✍ Scribed by Gierut, J. A.; Sowa, F. J.; Nieuwland, J. A.

Book ID
127072672
Publisher
American Chemical Society
Year
1936
Tongue
English
Weight
208 KB
Volume
58
Category
Article
ISSN
0002-7863

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RSiR;: The suspension of 1 in ether was treated with an excess (3.6 equivalents) of organometallic reagent. After the addition, the mixture was refluxed for 1 h and then hydrolyzed with H2S04 (25%). The silane was then extracted as described above.