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Optimizing TiO 2 -Based Phosphopeptide Enrichment for Automated Multidimensional Liquid Chromatography Coupled to Tandem Mass Spectrometry

✍ Scribed by Cantin, Greg T.; Shock, Teresa R.; Park, Sung Kyu; Madhani, Hiten D.; Yates, John R.

Book ID
127302926
Publisher
American Chemical Society
Year
2007
Tongue
English
Weight
224 KB
Volume
79
Category
Article
ISSN
0003-2700

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A high throughput mass spectrometry based method is described for the determination of the 5-HT receptor agonist 31100, and its desmethyl metabolite, in human plasma. Samples were extracted using the MicroLutem system of solid phase extraction in the '96 well' format, automated by means of a robotic