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Opening of an Aza-closo-dodecaborane to an Aza-nido-dodecaborate

✍ Scribed by Franc Meyer; Dr. Jens Müller; Prof. Peter Paetzold; Priv.-Doz. Roland Boese

Publisher
John Wiley and Sons
Year
1992
Tongue
English
Weight
405 KB
Volume
31
Category
Article
ISSN
0044-8249

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Triphosgene: an efficient carbonylating agent for liquid and solid-phase aza-peptide synthesis. Application to the synthesis of two aza-analogues of the AChR MIR decapeptide
✍ Frédéric André; Michel Marraud; Theodoros Tsouloufis; Socrates J. Tzartos; Guy B 📂 Article 📅 1997 🏛 John Wiley and Sons 🌐 English ⚖ 335 KB 👁 1 views

The N a aC a H exchange in aza-peptides has the advantage of preserving the side chain. Bis(trichloromethyl)carbonate or triphosgene is a solid, stable phosgene substitute which retains its high reactivity. Temperature and coupling times are greatly reduced with reference to other usually recommende