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One- to Three-Dimensional CuI and CuCN Based Coordination Polymers containing the Alkali Cation Ligating Thiacrown Ether 1, 10-Dithia-18-Crown-6

✍ Scribed by T. Röttgers; W. S. Sheldrick

Book ID: 101365447
Publisher: John Wiley and Sons
Year: 2002
Tongue: German
Weight: 195 KB
Volume: 628
Category: Article
ISSN: 0372-7874
DOI: 10.1002/1521-3749(200206)628:6<1305::aid-zaac1305>3.0.co;2-h

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The lamellar coordination polymer 2 R [CuI(1,10DT18C6)] (1) (1,10DT18C6 ‫؍‬ 1,10-dithia-18-crown-6) may be prepared by reaction of CuI with the thiacrown ether in acetonitrile. 1 crystallizes in the monoclinic space group P2 1 /n with a ‫؍‬ 10.764(2), b ‫؍‬ 14.317(3), and c ‫؍‬ 12.335(3) A > , ‫؍‬ 9