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One-step synthesis of 2,6-naphthalenedicarboxylic acid from naphthalene using cyclodextrin as catalyst

✍ Scribed by Hidefumi Hirai; Yukihide Shiraishi; Hiroaki Shirai

Publisher: John Wiley and Sons
Year: 1995
Tongue: English
Weight: 246 KB
Volume: 16
Category: Article
ISSN: 1022-1336
DOI: 10.1002/marc.1995.030160910

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✦ Synopsis

Abstract

The one‐step synthesis of 2,6‐naphthalenedicarboxylic acid from naphthalene with carbon tetrachloride, copper powder and aqueous alkali has been achieved under mild conditions by the use of β‐cyclodextrin as catalyst, producing 2,6‐naphthalenedicarboxylic acid in 65 mol‐% yield with 79% selectivity.

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