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One-step synthesis of 1-vinyl-2-thiabicyclo[3.2.0]hept-3-ene from vinylacetylene and hydrogen sulfide

โœ Scribed by B. A. Trofimov; G. A. Kalabin; S. V. Amosova; G. K. Musorin; V. V. Keiko; V. V. Kryuchkov

Book ID
112362086
Publisher
Springer US
Year
1976
Tongue
English
Weight
50 KB
Volume
12
Category
Article
ISSN
0009-3122

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1H and 13C NMR spectra of new 2-thiabicy
1H and 13C NMR spectra of new 2-thiabicyclo[3.2.0]hept-3-enes
โœ G. A. Kalabin; B. A. Trofimov ๐Ÿ“‚ Article ๐Ÿ“… 1978 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 358 KB

Three new compounds, one with the mo~ecular formula c6&s and hvo COmspOnding to GHloS have been isolated together with the main product, divinyl sulphide, from the reaction products of acetylene with sodium sulphide. Structure determination through 'H and 13C NMR with selective "C4'H) decoupling, sh