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One-Pot, Three-Component Synthesis of Linearly Substituted Homoallylic Alcohols via Allyl(isopropoxy)dimethylsilane

✍ Scribed by Li, Lianhai; Navasero, Neenah

Book ID
120337887
Publisher
American Chemical Society
Year
2004
Tongue
English
Weight
78 KB
Volume
6
Category
Article
ISSN
1523-7060

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General procedure: A flame-dried round-bottomed flask was charged with 4 (1 equiv) and the olefin cross partner (3.0 equiv). A rubber septum was attached, dichloromethane was added (0.2 Β± 0.3 n in 4), and argon was bubbled through the resultant solution for 10 min. Under a stream of argon, 3 (0.050