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One-Pot, Three-Component Synthesis of Linearly Substituted Homoallylic Alcohols via Allyl(isopropoxy)dimethylsilane.

✍ Scribed by Lianhai Li; Neenah Navasero

Book ID
101964240
Publisher
John Wiley and Sons
Year
2004
Weight
35 KB
Volume
35
Category
Article
ISSN
0931-7597

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General procedure: A flame-dried round-bottomed flask was charged with 4 (1 equiv) and the olefin cross partner (3.0 equiv). A rubber septum was attached, dichloromethane was added (0.2 Β± 0.3 n in 4), and argon was bubbled through the resultant solution for 10 min. Under a stream of argon, 3 (0.050