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One-Pot Three-Component Barbier-Type Reaction for the Synthesis of β-Nitroamines

✍ Scribed by Soengas, Raquel; Silva, Artur


Book ID
126511780
Publisher
Thieme Medical Publishers
Year
2013
Tongue
English
Weight
86 KB
Volume
24
Category
Article
ISSN
0936-5214

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Three-component one-pot reaction for the
✍ Yan-Ping Luo, Qiong Chen 📂 Article 📅 2013 🏛 Versita 🌐 English ⚖ 189 KB

## Abstract β-amide ketones were synthesised by a three-component one-pot reaction of phenylacetylene, aldehydes, and amides in anhydrous acetonitrile containing trifluoroacetic acid and acetic acid in the presence of AlCl3 catalyst. The title compound structures were identified by 1H NMR, 13C NMR,