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One-pot synthesis of selenocarbamates from isocyanates and diselenides using the Zn/AlCl3 system

โœ Scribed by Movassagh, Barahman; Moradi, Mona

Book ID
121501282
Publisher
Chinese Electronic Periodical Services
Year
2013
Tongue
English
Weight
181 KB
Volume
24
Category
Article
ISSN
1001-8417

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One-pot synthesis of ฮฒ-hydroxysulfides f
One-pot synthesis of ฮฒ-hydroxysulfides from styrenes and disulfides using the Zn/AlCl3 system
โœ Barahman Movassagh; Mozhgan Navidi ๐Ÿ“‚ Article ๐Ÿ“… 2008 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 161 KB

A simple, general, and highly regioselective procedure has been developed for the one-pot synthesis of b-hydroxysulfides in good yields from various styrenes and disulfides by cleavage of the S-S bond with a Zn/AlCl 3 system in aqueous acetonitrile at 80 ยฐC and in the presence of oxygen.