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One-dimensional Chain Crown Ether Complexes. Synthesis and Crystal Structure of Benzo-18-Crown 6 Complexes with Na2[M(SCN)4] (M = Pd, Pt)

✍ Scribed by Da-Cheng Li; Zeng-Xin Li; Jian-Min Dou; Da-Qi Wang


Book ID
111552515
Publisher
Springer Netherlands
Year
2003
Tongue
English
Weight
222 KB
Volume
46
Category
Article
ISSN
0923-0750

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For both structures all hydrogens were located in difference Fourier syntheses. The structures were refined by least-squares methods (OWLS ' ' 1 ; scale factor, isotropic extinction parameter, position parameters, anisotropic thermal parameters for non-Hatoms, isotropic thermal parameters for H) to