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On the determination of traces of organic bases in benzol and the like

✍ Scribed by Wiison, H. N.


Publisher
Wiley (John Wiley & Sons)
Year
1948
Weight
267 KB
Volume
67
Category
Article
ISSN
0368-4075

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✦ Synopsis


Abstract

A method is described for the determination of traces of basic nitrogen in hydrocarbons and the like by titration with perchloric acid in glacial acetic acid in the complete absence of water. Enough glacial acetic acid is added to the sample to keep perchlorates of bases in solution, and methyl violet is used as indicator.


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A method for the rapid determination of
✍ Robert H. White; Lowell P. Hager πŸ“‚ Article πŸ“… 1977 πŸ› Elsevier Science 🌐 English βš– 290 KB

Analytical methods have been developed for the rapid determination of trace lipid-soluble organic halogenated compounds in biological materials. Biological samples are extracted with a methanol-toluene mixture and, after partitioning with water to remove the inorganic halogens, the resulting toluene