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A method for the rapid determination of trace organic halogens in lipids

โœ Scribed by Robert H. White; Lowell P. Hager


Publisher
Elsevier Science
Year
1977
Tongue
English
Weight
290 KB
Volume
78
Category
Article
ISSN
0003-2697

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โœฆ Synopsis


Analytical methods have been developed for the rapid determination of trace lipid-soluble organic halogenated compounds in biological materials. Biological samples are extracted with a methanol-toluene mixture and, after partitioning with water to remove the inorganic halogens, the resulting toluene layers are assayed for their halogen content. A specifically designed instrument is described for the determination of total halogens (Cl, Br, and I) and the bromine content of these toluene extracts. Lipid-soluble organic halogen concentrations down to 1 &g wet weight of tissue were routinely assayed by the methods described.


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