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On-line NMR detection of microgram quantities of heparin-derived oligosaccharides and their structure elucidation by microcoil NMR

✍ Scribed by Albert K. Korir; Cynthia K. Larive


Publisher
Springer
Year
2007
Tongue
English
Weight
350 KB
Volume
388
Category
Article
ISSN
1618-2650

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Isolation and charaterization of hexasac
✍ Anni Larnkjaer; Svend Hoeime Hansen; Per Bjoern Østergaard πŸ“‚ Article πŸ“… 1995 πŸ› Elsevier Science 🌐 English βš– 792 KB

Four hexasaccharides representing major structural sequences of heparin were isolated and characterized after degradation of heparin by heparinase. The structures were determined from two-dimensional 1H NMR spectroscopy including TOCSY (total correlated spectroscopy), COSY (correlated spectroscopy),