First Insertion Reaction of Carbon Monox
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Prof. Dr. Ekkehard Lindner; Dipl.-Chem. GΓΌnter von Au
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Article
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1980
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John Wiley and Sons
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English
β 229 KB
A solution of ( I l i ) (10 g, 19.3 mmol) in 80 ml of anhydrous toluene, which contains 5 ml ethanol, is heated under reflux for 12 h. The solvent is removed and the residue digested with 50 ml pentane. Precipitated Ph3P0 is separated off and the previously unknown 4,5,6,6a-tetrahydro-2( 1 H)-pental