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Oligomers with four 3,4-quinolinediyl units and α,ω-bis (4-chloro-3-quinolinylthio)alkanes

✍ Scribed by Stanislaw Boryczka; Magdalena Rudnik; Andrzej Maślankiewicz

Book ID
112131440
Publisher
Journal of Heterocyclic Chemistry
Year
1996
Tongue
English
Weight
338 KB
Volume
33
Category
Article
ISSN
0022-152X

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α,ω-Bis(4-substituted-3-quinolinylthio)a
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## Abstract The reaction of thioquinanthrene 1 with sodium alkoxides and α,ω‐dihaloalkanes leads to the formation of α,ω‐bis[4‐(4‐methoxy‐3‐quinolinylthio)‐3‐quinolinylthio]alkanes 4. The yield depends on the nature of α,ω‐dihalo‐alkanes. The effect of α,ω‐dihaloalkanes of the following types: XCH~

13C NMR studies of α,ω-bis(p-anisyl)alka
13C NMR studies of α,ω-bis(p-anisyl)alkanes and α,ω-bis(3-iodo-4-methoxyphenyl)alkanes
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## Abstract ^13^C NMR studies were performed for a series of homologous iodinated and uniodinated α,ω‐bis(aryl)alkanes. Spectral assignments were made by utilization of DQCOSY, HETCOR‐LR and 1D coupled and decoupled ^13^C experiments.