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13C NMR studies of α,ω-bis(p-anisyl)alkanes and α,ω-bis(3-iodo-4-methoxyphenyl)alkanes

✍ Scribed by Gary L. Asleson; Kelly K. Catlin; Frederick J. Heldrich

Publisher
John Wiley and Sons
Year
1992
Tongue
English
Weight
264 KB
Volume
30
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

^13^C NMR studies were performed for a series of homologous iodinated and uniodinated α,ω‐bis(aryl)alkanes. Spectral assignments were made by utilization of DQCOSY, HETCOR‐LR and 1D coupled and decoupled ^13^C experiments.

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✍ Stanislaw Boryczka 📂 Article 📅 1998 🏛 Journal of Heterocyclic Chemistry 🌐 English ⚖ 433 KB

## Abstract The reaction of thioquinanthrene 1 with sodium alkoxides and α,ω‐dihaloalkanes leads to the formation of α,ω‐bis[4‐(4‐methoxy‐3‐quinolinylthio)‐3‐quinolinylthio]alkanes 4. The yield depends on the nature of α,ω‐dihalo‐alkanes. The effect of α,ω‐dihaloalkanes of the following types: XCH~