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O-(2,3,4,5,6-Penta­fluoro­benzyl)­hydroxy­laminium chloride

✍ Scribed by Gdaniec, Maria

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
143 KB
Volume
61
Category
Article
ISSN
1600-5368

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2,3,4,5,6-Penta­fluoro­benz­amide
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✍ Gdaniec, Maria 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 200 KB

Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.002 A Ê R factor = 0.035 wR factor = 0.090 Data-to-parameter ratio = 11.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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Molecules of the title compound, [Rh(C 9 H 6 NO)(C 18 F 15 P)-(CO)], pack in a tail-to-tail fashion, with an intermolecular ligand-to-ligandstacking distance of 3.399 (8) A ˚. The effective cone angle (Â E ) for the phosphine ligand is 163 . The bite angle of the bidentate oxine ligand is 80.77 (10)

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The tetrahydropyrimidine ring of the title molecule, C 11 H 11 FN 2 OS, adopts a half-chair conformation. In the crystal structure, the molecules are linked to form centrosymmetric hydrogen-bonded dimers.