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Nuclear magnetic resonance spectra of bridgehead diazabicyclo[3.3.1]nonanes and -[3.2.1]octanes and adamantanes. Effects of alkyl substitution

✍ Scribed by Nelsen, Stephen F.; Hintz, P. J.; Landis, R. T.

Book ID
126802316
Publisher
American Chemical Society
Year
1972
Tongue
English
Weight
406 KB
Volume
94
Category
Article
ISSN
0002-7863

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Conformation in solution of tetraaryl-3,7-diazabicyclo[3.3.1]-nonanes and tetra- and pentaaryl-1,3-diazaadamantanes. A nuclear magnetic resonance study
✍ Jackman, Lloyd M. ;Dunne, Theresa S. ;MΓΌller, Bodo ;Quast, Helmut πŸ“‚ Article πŸ“… 1982 πŸ› Wiley (John Wiley & Sons) 🌐 English βš– 947 KB

The proton NMR spectra of a series of tetraaryl-3,7-diazabicyclo[3.3.l]nonanes, 5 -12, have been assigned with the aid of nuclear Overhauser difference spectroscopy. The NOE's together with spin lattice relaxation times have been used to show that these molecules adopt the chair-boat conformation wi